Diffusion and Electrophoretic NMR

Peter Stilbs

Published by De Gruyter 2019

Diffusion and Electrophoretic NMR

Peter Stilbs

In the series De Gruyter STEM

https://doi.org/10.1515/9783110551532

Overview
Contents

About this book

Diffusion and Eletrophoretic NMR experiments resolve chemical compounds based on their molecular motion. This publication introduces the basics of these methods and explains how they can be used to measure the size of molecules and aggregates, to determine degree of polymerization and to solve other chemical problems. Supplied with many case studies, the book is a must-have for students and researchers who work with practical NMR measurements.

Gives an overview how to perform practical measurents.
Explains the principles of diffusion and electrophoretic NMR spectra interpretation.
Suitable for students with basic NMR knowledge.

Author / Editor information

Prof. Dr. Peter Stilbs, Royal Institute of Technology (KTH), Stockholm, Sweden.

Supplementary Materials

CORE Distribution 2019

Topics

Frontmatter Publicly Available Download PDF	I
Preface Publicly Available Download PDF	V
Contents Publicly Available Download PDF	IX
About the Author Publicly Available Download PDF	XVIII
1. Historical perspectives and basic pulsed NMR concepts Requires Authentication Unlicensed Licensed Download PDF	1
2. Basic concepts Requires Authentication Unlicensed Licensed Download PDF	30
3. PGSE NMR diffusometry example applications Requires Authentication Unlicensed Licensed Download PDF	100
4. Getting started Requires Authentication Unlicensed Licensed Download PDF	155
5. Nonobvious pitfalls and other potentially confusing elements in PGSE studies Requires Authentication Unlicensed Licensed Download PDF	175
6. Data preparation, evaluation and presentation Requires Authentication Unlicensed Licensed Download PDF	195
7. Specialized measurements and systems Requires Authentication Unlicensed Licensed Download PDF	250
8. Electrophoretic NMR (eNMR) Requires Authentication Unlicensed Licensed Download PDF	266
9. Building home-brew PGSE and eNMR instrumentation Requires Authentication Unlicensed Licensed Download PDF	303
10. Other more recent texts and reviews on NMR diffusometry Requires Authentication Unlicensed Licensed Download PDF	315
Appendix: Quantifying self-diffusion-related spin echo magnetic field gradient-induced spin echo attenuation and deriving the basic pulsed-gradient Stejskal–Tanner relation Requires Authentication Unlicensed Licensed Download PDF	318
Index Requires Authentication Unlicensed Licensed Download PDF	323

(Deutsch)

Language: English
Publisher: De Gruyter
Audience: Students, Analytical Chemists, Organic Chemists, researchers & professionals who work with practical NMR measurements.
Pages
- Front matter: 18
- Main content: 332
Illustrations
- Illustrations: 178
- Coloured Illustrations: 22
- Tables: 2
Keywords: Analytical Chemistry; Chemical Analysis; NMR Spectroscopy.

eBook

Published: August 19, 2019
ISBN: 9783110551532

Paperback

Published: August 19, 2019
ISBN: 9783110551525